Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chlorobenzyl mercaptan → Emd 39593
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chlorobenzyl mercaptan | HCID 580759 | — |
| 반응물 | 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine | HCID 948792 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Emd 39593 | HCID 135146 | — |
반응 단계
2.76 g of Na is dissolved in 180 ml of ethanol; 19.1 g of o-chlorobenzylmercaptan and 16.76 g of 4-chloro-1-methyl-1H-imidazo(4,5-c)pyridine are added; the mixture is boiled for 16 hours and evaporated; and the residue is worked up in the customary manner to give 4-o-chloro-benzylthio-1-methyl-1H-imidazo(4,5-c)pyridine of m.p. 152°-155° (from ethanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04654350 |
| 출처 데이터셋 | uspto-grants-1987_03 |
| ORD ID | ord-356079d3f1214307a783e51e9d01b193 |
| 출처 메모 | uspto-grants-1987_03 |