3-methoxy-6-methyl-4-nitropyridazine 1-oxide → HCID 21766149, 화합물

HRID 1907822노트

반응식

HRID 1907822 반응식
[CH3:1][O:2][C:3]1[N:4]=[N+:5]([O-:13])[C:6]([CH3:12])=[CH:7][C:8]=1[N+]([O-])=O.[CH3:14][O-:15].[Na+]>CO>[CH3:1][O:2][C:3]1[N:4]=[N+:5]([O-:13])[C:6]([CH3:12])=[CH:7][C:8]=1[O:15][CH3:14]

참가 물질

4

반응물 2

HCID 64053053-methoxy-6-methyl-4-nitropyridazine 1-oxideHCID 10942334Sodium Methoxide

생성물 1

HCID 21766149HCID 21766149, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

3-Methoxy-6-methyl-4-nitropyridazine 1-oxide (1 g) was converted and worked up analogously to example 1 g). Chromatography of the crude product was unnecessary. The solvent used was methanol (30 ml), and the base sodium methoxide (as 30% solution in methanol, 1.1 ml). Yield: 900 mg LC-MS Rt: 0.29 min [M+H]+:171.1

출처 및 근거

ORD 기록
ord-73fa67287c55470cb6a518fcc5adc71e
출처 데이터셋
uspto-grants-2013_12
특허 번호
US08598177B2

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