Methyl 4-amino-5-nitropyridine-2-carboxylate → Methyl 4,5-diaminopicolinate
반응식
[CH3:1][O:2][C:3](=[O:14])[C:4]1[CH:9]=[C:8]([NH2:10])[C:7]([N+:11]([O-])=O)=[CH:6][N:5]=1>C1COCC1.[Pd]>[NH2:10][C:8]1[C:7]([NH2:11])=[CH:6][N:5]=[C:4]([C:3]([O:2][CH3:1])=[O:14])[CH:9]=1참가 물질
4
실험 절차
Prepared analogously to example 83d by hydrogenation of methyl-4-amino-5-nitropicolinate using palladium/charcoal 10% in THF.
출처 및 근거
- ORD 기록
- ord-27962eb3ad594589bff808d237e2923a
- 출처 데이터셋
- uspto-grants-2013_12
- 특허 번호
- US08598190B2
반응 노트
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