Triethylsilane → HCID 69000417, 화합물

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[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:13][C:12]([CH:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)O)=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.C([SiH](CC)CC)C>>[CH2:14]([C:12]1[S:13][C:9]([C:6]2[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=2)=[CH:10][CH:11]=1)[C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1

참가 물질

반응물 2

HCID 12052Triethylsilane

HCID 68998767HCID 68998767, 화합물

생성물 1

HCID 69000417HCID 69000417, 화합물수율 99%

실험 절차

The title compound was prepared from the product of step 2 (0.6 g, 2.0 mmol) and triethylsilane (2.4 g, 20.2 mmol) using the procedure of Example 159, step 3 with 99% yield (0.55 g).

출처 및 근거

ORD 기록: ord-b4a19e90e0e849de87ffac856379952a
출처 데이터셋: uspto-grants-2013_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08598359B2

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