2-Hydrazinopyridine → HCID 178515580, 화합물

HRID 1911916노트

반응식

HRID 1911916 반응식
[F:1][C:2]([F:18])([F:17])[C:3]1[CH:4]=[C:5]([CH:14]=[CH:15][CH:16]=1)[C:6]([CH2:8][C:9]([O:11]CC)=O)=O.[NH:19]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][N:22]=1)[NH2:20]>C(O)C>[N:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:21]=1[N:19]1[C:9]([OH:11])=[CH:8][C:6]([C:5]2[CH:14]=[CH:15][CH:16]=[C:3]([C:2]([F:1])([F:17])[F:18])[CH:4]=2)=[N:20]1

참가 물질

4

반응물 2

HCID 786452-HydrazinopyridineHCID 2063905Ethyl 3-oxo-3-[3-(trifluoromethyl)phenyl]propanoate

생성물 1

HCID 178515580HCID 178515580, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매2회

실험 절차

Ethyl 3-trifluoromethylbenzoylacetate (10 mmol, manufactured by Aldrich) and ethanol (10 mL) were charged in a 100 mL round-bottom flask to which a solution of 2-hydrazinopyridine (10 mmol, manufactured by Aldrich) in ethanol (10 mL) was then added.

후처리

  1. additionwas then added

출처 및 근거

ORD 기록
ord-f2dd1734593b41cdbebfd4de2a34f6a8
출처 데이터셋
uspto-grants-2013_12
특허 번호
US08604210B2

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