Silica → N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

HRID 1912241노트

반응식

HRID 1912241 반응식
C[CH2:2][CH2:3][CH2:4][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:6][CH2:7][CH2:8]C.[Si](=O)=O>>[CH3:8][CH2:7][CH2:6][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:4][CH2:3][CH3:2]

참가 물질

3

반응물 2

HCID 24261SilicaHCID 12357718N-(dibutylcarbamothioyl)-3,4,5-trimethoxybenzamide

생성물 1

HCID 12357717N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

실험 절차

A mixture of 90 parts by mass of PET obtained above and 10 parts by mass of silicon dioxide (“Silysia 445,” average particle size 2.5 μm, manufactured by Fuji Silysia Chemical Ltd.) was kneaded at 260° C. using a vented counter-rotation twin-axis extruder (L/D=35) with 30 mmφ, to prepare a PPT master (MS-4) containing 10% by mass of silicon dioxide.

후처리

  1. customwas kneaded at 260° C.

출처 및 근거

ORD 기록
ord-349e197454b24492b94b51c9c718043d
출처 데이터셋
uspto-grants-2013_12
특허 번호
US08609227B2

반응 노트

불러오는 중…