반응식
[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=O.[CH3:10][C:11](=O)[CH:12]=[CH2:13].[NH2:15][S:16]([C:19]1[CH:24]=[CH:23][C:22]([NH2:25])=[CH:21][CH:20]=1)(=[O:18])=[O:17]>>[CH3:10][C:11]1[N:25]([C:22]2[CH:23]=[CH:24][C:19]([S:16]([NH2:15])(=[O:17])=[O:18])=[CH:20][CH:21]=2)[C:5]([C:4]2[CH:3]=[C:2]([CH3:1])[CH:9]=[CH:8][CH:7]=2)=[CH:13][CH:12]=1참가 물질
4
실험 절차
Meta-methylbenzaldehyde and but-3-en-2-one were treated according to the procedure outlined in General Procedure C followed by subjecting the resulting product to conditions outlined in General Procedure D along with p-aminosulfonyl phenylamine to obtain the titled compound. 1H NMR (CDCl3) δ ppm 2.15 (3H), 2.05 (3H), 4.90 (2H), 6.10 (1H), 6.30 (1H), 6.89-7.90 (8H); MS (ESI) m/z 327 (M+H).
출처 및 근거
- ORD 기록
- ord-e00edf77363b40f1a58c6448e9b888e8
- 출처 데이터셋
- uspto-grants-2013_12
- 특허 번호
- US08609713B2
연결된 노트
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