Sulfuryl chloride → HCID 19067199, 화합물

HRID 1913540노트

반응식

[CH3:1][CH:2]([CH3:14])[C:3]([O:5][CH:6]([O:8][C:9](SCC)=[O:10])[CH3:7])=[O:4].S(Cl)([Cl:18])(=O)=O>>[CH3:1][CH:2]([CH3:14])[C:3]([O:5][CH:6]([O:8][C:9]([Cl:18])=[O:10])[CH3:7])=[O:4]

참가 물질

반응물 2

HCID 24648Sulfuryl chloride

HCID 858856631-{[(Ethylthio)carbonyl]oxy}ethyl 2-methylpropionate

생성물 1

HCID 19067199HCID 19067199, 화합물

실험 절차

1-{[(Ethylthio)carbonyl]oxy}ethyl 2-methylpropionate (WO2005/66122) (412 mg) was cooled to −30° C. Sulfuryl chloride (157 μl) was added thereto, and the mixture was then stirred for 45 minutes. The solvent in the reaction solution was distilled off under reduced pressure to obtain a crude product of the title compound.

후처리

distillationThe solvent in the reaction solution was distilled off under reduced pressure

출처 및 근거

ORD 기록: ord-4c9388d3f6914b59bd6bf7ca6ed00553
출처 데이터셋: uspto-grants-2013_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08609710B2

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