Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine → 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine | HCID 22041340 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine | HCID 22041328 | — |
반응 단계
The mixture containing 2-nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine in methanol with catalytic amount of 10% Pd/C was hydrogenated until disappearance of yellow color to yield 4-(4-(3-pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine. MS: MH+=279.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08614330B2 |
| 출처 데이터셋 | uspto-grants-2013_12 |
| ORD ID | ord-8ed5c1b25eb64513822f2276de211d21 |
| 출처 메모 | uspto-grants-2013_12 |