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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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GlyTouCan:G06186NU → L-glucose monohydrate

HRID 1916032
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HRID 1916032 반응식
[O:1]=[CH:2][C@H:3]([C@@H:5]([C@H:7]([C@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4]>O>[OH2:1].[O:1]=[CH:2][C@H:3]([C@@H:5]([C@H:7]([C@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4]
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참가 물질

3

반응물 1

HCID 10954115GlyTouCan:G06186NU

생성물 1

HCID 86651444L-glucose monohydrate

시약·촉매·용매 1

HCID 962Water용매3회

실험 절차

In another embodiment, the process comprises: a) dispersing an amount from about 0.9 moles per liter to about 1.5 moles per liter of a source of L-glucose in water at a temperature of from about 55° C. to not more than about 65° C. at a reduced pressure of at least about 700 mm Hg less than atmospheric pressure, reducing the amount of water present such that the amount of water present is from about 28% to about 30% by weight of the solution, and heating the dispersion to a temperature of from about 80° C. to about 82° C. to form a solution; and b) cooling the solution to a temperature of from about 50° C. to about 55° C. to induce crystallization, further cooling the resulting slurry to a temperature of from about 25° C. to about 30° C., and adding an amount of ethanol that is from about 4.5 mL of ethanol to about 5 mL of ethanol per gram of L-glucose dispersed in step (a) to form L-glucose monohydrate.

후처리

  1. temperatureheating the dispersion to a temperature of from about 80° C. to about 82° C.
  2. customto form a solution
  3. temperatureand b) cooling the solution to a temperature of from about 50° C. to about 55° C.
  4. customcrystallization
  5. temperaturefurther cooling the resulting slurry to a temperature of from about 25° C. to about 30° C.
  6. additionadding an amount of ethanol that
  7. additiondispersed in step (a)

출처 및 근거

ORD 기록
ord-e4b41803e5584ea9ad0519df96006cdb
출처 데이터셋
uspto-grants-2013_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08618067B2

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