Potassium Carbonate → Ethyl 4-(benzyloxy)-3-hydroxybenzoate

HRID 1918318노트

반응식

HRID 1918318 반응식
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

참가 물질

4

반응물 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, 화합물

생성물 1

HCID 11311797Ethyl 4-(benzyloxy)-3-hydroxybenzoate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The compound of step 2 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. The solution was evaporated to dryness and the residue used without further purification.

후처리

  1. temperatureunder reflux
  2. customThe solution was evaporated to dryness
  3. customthe residue used without further purification

출처 및 근거

ORD 기록
ord-8b32513e163d4143a66e1a137d6b959b
출처 데이터셋
uspto-grants-2013_12
특허 번호
US08618304B2

반응 노트

불러오는 중…