5,7-Dichloro-2-methylthiazolo[5,4-d]pyrimidine → 5,7-Dichloro-2-methylthiazolo[4,5-d]pyrimidine

HRID 1919358노트

반응식

HRID 1919358 반응식
[Cl:1][C:2]1[N:3]=[C:4]([Cl:12])[C:5]2N=C(C)S[C:6]=2[N:7]=1.[CH3:13][C:14]1[S:15]C2C(=O)NC(=O)NC=2[N:24]=1>>[Cl:1][C:2]1[N:3]=[C:4]([Cl:12])[C:5]2[S:15][C:14]([CH3:13])=[N:24][C:6]=2[N:7]=1

참가 물질

3

반응물 2

HCID 3456395,7-Dichloro-2-methylthiazolo[5,4-d]pyrimidineHCID 3456412-Methylthiazolo[4,5-d]pyrimidine-5,7(4H,6H)-dione

생성물 1

HCID 582349525,7-Dichloro-2-methylthiazolo[4,5-d]pyrimidine

실험 절차

Prepared using the method used in the preparation of 5,7-dichloro-2-methyl-thiazolo[5,4-d]pyrimidine using 2-methyl-4H-thiazolo[4,5-d]pyrimidine-5,7-dione in place of 2-methyl-4H-thiazolo[5,4d]pyrimidine-5,7-dione. The title compound was obtained as an solid solid (140 mg, 28%).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-1a0a22a048d94bfc99d1d4935974656f
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08168633B2

반응 노트

불러오는 중…