3-Fluoro-4-methylphenylhydrazine → HCID 46220047, 화합물

반응식

C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=2)[N:8]=1)=O.[F:26][C:27]1[CH:28]=[C:29]([NH:34]N)[CH:30]=[CH:31][C:32]=1[CH3:33]>>[F:26][C:27]1[CH:28]=[C:29]([N:34]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:30]=[CH:31][C:32]=1[CH3:33]

참가 물질

반응물 2

HCID 27746313-Fluoro-4-methylphenylhydrazine

HCID 593701233-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

생성물 1

HCID 46220047HCID 46220047, 화합물

실험 절차

Reaction of 3-((E)-3-dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-6) and (3-fluoro-4-methyl-phenyl)-hydrazine according to example 43 gave the desired product. MS: M=431.0 (M+H)+

출처 및 근거

ORD 기록: ord-1cb0955f4e414094bd6bf53cf23beba2
출처 데이터셋: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08178538B2

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