3-Fluoro-4-methylphenylhydrazine → HCID 59369974, 화합물

반응식

C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([S:20]([CH3:23])(=[O:22])=[O:21])[CH:15]=2)[N:8]=1)=O.[F:25][C:26]1[CH:27]=[C:28]([NH:33]N)[CH:29]=[CH:30][C:31]=1[CH3:32]>>[F:25][C:26]1[CH:27]=[C:28]([N:33]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[C:16]([S:20]([CH3:23])(=[O:22])=[O:21])[CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:29]=[CH:30][C:31]=1[CH3:32]

참가 물질

반응물 2

HCID 27746313-Fluoro-4-methylphenylhydrazine

HCID 593701713-((E)-3-Dimethylamino-acryloyl)-1-(3-methansulfonyl-phenyl)-1H-pyridazin-4-one

생성물 1

HCID 59369974HCID 59369974, 화합물

실험 절차

Reaction of 3-((E)-3-dimethylamino-acryloyl)-1-(3-methansulfonyl-phenyl)-1H-pyridazin-4-one (A-7) and (3-fluoro-4-methyl-phenyl)-hydrazine according to example 43 gave the desired product. MS: M=425.3 (M+H)+

출처 및 근거

ORD 기록: ord-e4870d286a9f48a8acfb86332302b99b
출처 데이터셋: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08178538B2

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