4-Bromo-1,3-benzothiazol-2-amine → 2-Aminobenzo[d]thiazole-4-carbonitrile

HRID 1926436노트

반응식

HRID 1926436 반응식
[NH2:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[C:7](Br)[C:5]=2[N:6]=1.[C:12]([Cu])#[N:13]>CN(C=O)C>[NH2:1][C:2]1[S:3][C:4]2[C:5](=[C:7]([C:12]#[N:13])[CH:8]=[CH:9][CH:10]=2)[N:6]=1

참가 물질

4

반응물 2

HCID 20498884-Bromo-1,3-benzothiazol-2-amineHCID 178418546HCID 178418546, 화합물

생성물 1

HCID 221525632-Aminobenzo[d]thiazole-4-carbonitrile

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

The title compound was prepared from 2-amino-4-bromo-1,3-benzothiazole by heating with CuCN (1.0 eq.) in DMF at 160° C. for 12 h.

출처 및 근거

ORD 기록
ord-32dc9fde2c84460f8840becf468d7d1e
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08178668B2

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