HCID 57468627, 화합물 → HCID 57468807, 화합물

HRID 1927949노트

반응식

HRID 1927949 반응식
Br[C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)[N:3]=1.[I:16][C:17]1[N:18]=[CH:19][NH:20][CH:21]=1>>[Cl:15][C:12]1[CH:13]=[CH:14][C:9]([C:4]2[CH:5]=[C:6]([CH3:8])[CH:7]=[C:2]([N:20]3[CH:21]=[C:17]([I:16])[N:18]=[CH:19]3)[N:3]=2)=[CH:10][CH:11]=1

참가 물질

3

반응물 2

HCID 57468627HCID 57468627, 화합물HCID 178506559HCID 178506559, 화합물

생성물 1

HCID 57468807HCID 57468807, 화합물

실험 절차

The title compound was prepared from 2-bromo-6-(4-chloro-phenyl)-4-methyl-pyridine (example A.22) (0.94 g, 3.0 mmol) and commercially available 4-iodo-imidazole (0.71 g, 3.3 mmol) according to the general procedure IVa. Obtained as a yellow gum (0.213 g, 18%). MS (ISP) 396.0 [(M+H)+].

출처 및 근거

ORD 기록
ord-dd0af26408b9487abcc155e8c43c51c2
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08183262B2

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