Malonic acid, disodium salt → Zinc Malonate Dihydrate

HRID 1928694

반응식

HRID 1928694 반응식
O.O.N[C@H](C([O-])=O)CCC([O-])=[O:8].[Zn+2:13].C([O-])(=O)CC([O-])=[O:17].[Na+].[Na+].[CH2:23]([C:27]([O-:29])=[O:28])[C:24]([O-:26])=[O:25].[Cl-].[Zn+2].[Cl-]>O>[OH2:8].[OH2:17].[C:27]([O-:29])(=[O:28])[CH2:23][C:24]([O-:26])=[O:25].[Zn+2:13]

참가 물질

6

반응물 4

HCID 8865Malonic acid, disodium saltHCID 9084Malonate IonHCID 3007855ZincchlorideHCID 22825209Zinc L-glutamate Dihydrate

생성물 1

HCID 86616729Zinc Malonate Dihydrate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Basically the reaction conditions found for preparation of zinc L-glutamate (Example 13) was employed. A suspension of sodium malonate (white coloured) is prepared by adding 100 mL of millipore water to 16.605 g (0.1 moles) of solid sodium malonate dibasic monohydrate (SIGMA M1875-100G, MW 166.05, CAS 26522-85-0) in a 250 mL beaker. To this suspension was added 13.628 g (0.1 moles) of solid zinc chloride (FLUKA, 96469, MW 136.3, CAS 7646-85-7). Subsequent manufacturing steps were as described in Example 13.

후처리

  1. customBasically the reaction conditions
  2. customis prepared

출처 및 근거

ORD 기록
ord-0472fd44f35a4480b7a4ceff7a3e455e
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08183409B2

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