Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Bromoisatin → HCID 178504804, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Bromoisatin | HCID 6889 | — |
| 반응물 | 4-(Methylsulphonyl)phenylhydrazine | HCID 70142 | — |
| 생성물 | HCID 178504804 | HCID 178504804 | 72% |
반응 단계
The title compound was prepared in 72% yield from 5-bromo-1H-indole-2,3-dione (Meth-Cohn and Goon, Tetrahedron Letters 1996, 37, 9381-14) and 4-methylsulfonylphenylhydrazine according to Procedure G: 1H NMR (DMSO-d6): δ 12.7 (s, 1H), 11.3 (s, 1H), 7.9 (d, 2H), 7.7-7.8 (m, 3H), 7.4 (dd,1H), 6.9 (d, 1H), 3.2 (s, 3H); ESI−MS m/z 392 (M−H)−.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06387919B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-f43fd3eb4d0e420bbde2178933580c1d |
| 출처 메모 | uspto-grants-2002_05 |