5-Methoxyisatin → HCID 178487247, 화합물

HRID 1935527

반응식

HRID 1935527 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][C:7](=[O:12])[C:6]2=O.Cl.[NH:15]([C:17]1[CH:22]=[CH:21][C:20]([S:23]([NH2:26])(=[O:25])=[O:24])=[CH:19][CH:18]=1)[NH2:16]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][C:7](=[O:12])[C:6]2=[N:16][NH:15][C:17]1[CH:22]=[CH:21][C:20]([S:23]([NH2:26])(=[O:24])=[O:25])=[CH:19][CH:18]=1

참가 물질

3

반응물 2

HCID 383335-MethoxyisatinHCID 27945674-Hydrazinylbenzenesulfonamide hydrochloride

생성물 1

HCID 178487247HCID 178487247, 화합물

실험 절차

The title compound was prepared from 5-methoxy-1H-indole-2,3-dione (Gassman, et al., Journal of Organic Chemistry 1977, 42, 1344-8) and 4-hydrazino benzenesulfonamide hydrochloride according to Procedure G: mp >250° C; 1H NMR (DMSO-d6): δ 3.80 (s, 3H), 6.87 (s, 2H), 7.20 (s, 1H), 7.28 (s, 2H), 7.60 (d, J=8.8 Hz, 2H), 7.81 (d, J=8.8 Hz, 2H), 10.93 (s, 1H), 12.85 (s, 1H); APCI−MS m/z 344.9 (M−H)−.

출처 및 근거

ORD 기록
ord-e7a3528c308b43028d7b576c5a1151f3
출처 데이터셋
uspto-grants-2002_05
특허 번호
US06387919B1

연결된 노트

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