Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid → 3-(4-Methoxyphenyl)-2-phenylpropionic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid | HCID 236698 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 3-(4-Methoxyphenyl)-2-phenylpropionic acid | HCID 97739 | — |
반응 단계
Palladium on activated carbon (10% wt., 2.77 g) was added to a solution of 3-(4-methoxyphenyl)-2-phenylacrylic acid (27.7 g, 0.11 mol) in acetic acid (1000 ml). The mixture was hydrogenated at ambient temperature. The mixture was filtered through Celite, and the solvent was evaporated. The product was recrystallized from a small amount of ethyl acetate. Melting point 220-221° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06388090B2 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-1882dce487974d0793678a129d3179de |
| 출처 메모 | uspto-grants-2002_05 |