Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-(4-Methoxyphenyl)-2-phenylpropionyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-(4-Methoxyphenyl)-2-phenylpropionic acid | HCID 97739 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-(4-Methoxyphenyl)-2-phenylpropionyl chloride | HCID 11140323 | — |
반응 단계
3-(4-Methoxyphenyl)-2-phenylpropanoic acid (12.5 g, 0.049 mol) was converted to its acid chloride by treatment with thionyl chloride (8.2 ml) in dry dichloromethane (75 ml) at 40° C. Excess thionyl chloride and dichloromethane were evaporated off. The crude product was used in the next step without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06388090B2 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-8330fac80b4f466ab997698fb37b3886 |
| 출처 메모 | uspto-grants-2002_05 |