N-benzyl-6-(4-phenylbutoxy)hexan-1-amine → 6-(4-Phenylbutoxy)hexan-1-amine
반응식
C([NH:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][O:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)C1C=CC=CC=1>CCO.[Pd]>[C:20]1([CH2:19][CH2:18][CH2:17][CH2:16][O:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][NH2:8])[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1참가 물질
4
실험 절차
A solution of 4.02 g (11.86 mmol) N-benzyl-6-(4-phenylbutoxy)hexylamine in 40 ml EtOH is hydrogenated at room temperature and atmospheric pressure with 0.4 g 5% Pd/C. When 300 ml H2 have been absorbed, the mixture is filtered on decalite and the filtrate is concentrated to yield 2.89 g (97.9%) 6-(4-phenylbutoxy)hexylamine as an oil.
후처리
- customis hydrogenated at room temperature
- customWhen 300 ml H2 have been absorbed
- filtrationthe mixture is filtered on decalite
- concentrationthe filtrate is concentrated
출처 및 근거
- ORD 기록
- ord-f81998c366584b50bb1ceae388beb513
- 출처 데이터셋
- uspto-grants-2002_05
- 특허 번호
- US06388134B1
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