2-Ethoxybenzoyl chloride → HCID 22462351, 화합물

반응식

[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=1[C:6](Cl)=[O:7])[CH3:2].[NH2:13][C:14]1[C:15]([C:20]([NH2:22])=[O:21])=[N:16][CH:17]=[CH:18][CH:19]=1>>[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=1[C:6]([NH:13][C:14]1[C:15]([C:20]([NH2:22])=[O:21])=[N:16][CH:17]=[CH:18][CH:19]=1)=[O:7])[CH3:2]

참가 물질

반응물 2

HCID 30163972-Ethoxybenzoyl chloride

HCID 132387253-Amino-pyridine-2-carboxylic acid amide

생성물 1

HCID 22462351HCID 22462351, 화합물

실험 절차

The title compound was prepared from 2-ethoxybenzoyl chloride and 3-aminopyridine-2-carboxamide (J. Chem. Soc., 1956, 1045) following the procedure of Preparation 7 and was obtained as an off-white solid (100%), m.p. 172-177° C.

후처리

customthe procedure of Preparation 7

출처 및 근거

ORD 기록: ord-3db668fc4b774b8eb3789c44af949d98
출처 데이터셋: uspto-grants-2002_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06391885B1

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