Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triphosgene → HCID 22462550, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triphosgene | HCID 94429 | — |
| 반응물 | 4-(Pyridin-4-yl)naphth-1-ylamine | HCID 10857012 | — |
| 반응물 | 3-(1-Methylpiperidin-4-yl)-1h-indol-5-amine | HCID 11831220 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | HCID 22462550 | HCID 22462550 | — |
반응 단계
The title compound was prepared in a similar manner to Example 1 from 3-methyl-4-(pyridin-4-yl)aniline (prepared as for D3 from 4-bromo-3-methylaniline) (0.17 g, 0.9 mmole), 5-amino-3-(1-methylpiperdin-4-yl)-1H-indole (D2, 0.17 g, 0.75 mmole), triphosgene (0.10 g, 0.35 mmole) and triethylamine (0.07 ml). This was obtained as a buff powder (0.11 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06391891B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-bdc34677bf2a4cc1aaf411b119ecfb89 |
| 출처 메모 | uspto-grants-2002_05 |