Ammonia → HCID 22462467, 화합물

반응식

[N+:1]([C:4]1[CH:13]=[CH:12][C:11]2[NH:10][C:9](=S)[CH:8]3[CH2:15][CH2:16][CH2:17][CH:7]3[C:6]=2[CH:5]=1)([O-:3])=[O:2].[NH3:18]>>[NH2:18][C:9]1[CH:8]2[CH2:15][CH2:16][CH2:17][CH:7]2[C:6]2[CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:13]=[CH:12][C:11]=2[N:10]=1

참가 물질

반응물 2

HCID 222Ammonia

HCID 22462472HCID 22462472, 화합물

생성물 1

HCID 22462467HCID 22462467, 화합물수율 76%

실험 절차

As described for Example 4, 8-nitro-1,2,3,3a,5,9b-hexahydrocyclopenta[c]quinoline-4-thione (100 mg, 0.40 mmol) is reacted with 7N methanolic ammonia solution (15 ml) to form 70 mg (76%) of product.

출처 및 근거

ORD 기록: ord-03acb2bd3d794280b2bc5ecc8bd5069e
출처 데이터셋: uspto-grants-2002_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06391887B1

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