Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chlorooctane → Octyltrichlorosilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chlorooctane | HCID 8142 | — |
| 반응물 | Trichlorosilane | HCID 24811 | — |
| 촉매 | Tetrabutylphosphonium chloride | HCID 75311 | — |
| 생성물 | Octyltrichlorosilane | HCID 21354 | 85.2% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.20 g (0.68 mmol) of tetrabutylphosphonium chloride, 1.00 g (6.73 mmol) of 1-chlorooctane and 2.71 g (20.0 mmol) of trichlorosilane were reacted at 170° C. for 2 hrs. The resulting mixture was distilled to give 1.42 g of n-octyltrichlorosilane (yield; 85%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06392077B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-d8381254d70d4b2bb3357e2f5531e2a3 |
| 출처 메모 | uspto-grants-2002_05 |