Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trichloro(chloromethyl)silane → Bis(trichlorosilyl)methane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trichloro(chloromethyl)silane | HCID 15258 | — |
| 반응물 | Trichlorosilane | HCID 24811 | — |
| 반응물 | Benzyltributylphosphonium chloride | HCID 200231 | — |
| 생성물 | Bis(trichlorosilyl)methane | HCID 2756737 | 68% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.22 g (0.67 mmol) of benzyltributylphosphonium chloride, 1.23 g (6.69 mmol) of (chloromethyl)trichlorosilane, and 2.71 g (20.0 mmol) of trichlorosilane were reacted at 160° C. for 15 hrs. The resulting mixture was distilled to give 1.13 g of 1,1,1,3,3,3-hexachloro-1,3-disilapropane (yield; 68%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06392077B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-02059802c52946f29da4856f0cad71a8 |
| 출처 메모 | uspto-grants-2002_05 |