Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyldichlorosilane → Monophenethyldichlorosilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyldichlorosilane | HCID 6376 | — |
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | Benzyltributylphosphonium chloride | HCID 200231 | — |
| 생성물 | Monophenethyldichlorosilane | HCID 123907249 | 240.6% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.26 g (0.79 mmol) of benyltributylphosphonium chloride, 1.00 g (7.90 mmol) of benzyl chloride, and 2.73 g (23.7 mmol) of methyldichlorosilane were reacted at 200° C. for 2 hrs. The resulting mixture was distilled to give 0.39 g of benzylmethyldichlorosilane (yield; 24%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06392077B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-84c2b1619e68493395844cfc4bd26695 |
| 출처 메모 | uspto-grants-2002_05 |