Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Chloride → Benzene, [(trichlorosilyl)methyl]-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | Dichlorosilane | HCID 61330 | — |
| 반응물 | Benzyltributylphosphonium chloride | HCID 200231 | — |
| 생성물 | Benzene, [(trichlorosilyl)methyl]- | HCID 69863 | 53% |
| 생성물 | Benzyldichlorosilane | HCID 101943102 | 19% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.26 g (0.79 mmol) of benyltributylphosphonium chloride, 1.01 ml (7.98 mmol) of benzyl chloride, and 2.42 g (24.0 mmol) of dichlorosilane were reacted at 150° C. for 2 hrs. The resulting mixture was distilled to give 0.29 g of benzyldichlorosilane (yield; 19%) and 0.95 g of benzyltrichlorosilane (yield; 53%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06392077B1 |
| 출처 데이터셋 | uspto-grants-2002_05 |
| ORD ID | ord-380bfbcecc3d4ac1a46bb07f1b202964 |
| 출처 메모 | uspto-grants-2002_05 |