Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Isothiocyanato-3-(trifluoromethyl)benzene → N-(3-(trifluoromethyl)phenyl)-N'-(2-methoxy-5-(trifluoromethyl)phenyl) thiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Isothiocyanato-3-(trifluoromethyl)benzene | HCID 137232 | — |
| 반응물 | 2-Methoxy-5-(trifluoromethyl)aniline | HCID 600637 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-(3-(trifluoromethyl)phenyl)-N'-(2-methoxy-5-(trifluoromethyl)phenyl) thiourea | HCID 54197929 | 51% |
반응 단계
3-(trifluoromethyl)phenyl isothiocyanate in toluene (0.76 ml, 5.0 mmol) was added to a solution of 2-methoxy-5-(trifluoromethyl)aniline in toluene (10 ml). The resulting reaction mixture was stirred at RT overnight and the product was subsequently filtered off. 1.00 g (51%) of the title compound was isolated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05696138 |
| 출처 데이터셋 | uspto-grants-1997_12 |
| ORD ID | ord-0da55e70336c4445bca4d21c00860d8f |
| 출처 메모 | uspto-grants-1997_12 |