3-(4-ethylphenyl)prop-2-enoic Acid → 3-(4-ethylphenyl)propanoic Acid
반응식
[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH:7]=[CH:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]>[Pd].C(O)C>[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH2:7][CH2:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]참가 물질
4
실험 절차
An ethanol (250 ml) solution of 4-ethyl cinnamic acid (34.0 g, 0.191 mol) was hydrogenareal at 60 psi over 10% Pd/C (2 g) for 2 hr. The mixture was filtered and concentrated in vacuo to give 3-(4-ethylphenyl)propionic acid as a white solid (34 g, 100%).
후처리
- filtrationThe mixture was filtered
- concentrationconcentrated in vacuo
출처 및 근거
- ORD 기록
- ord-d7b8249b41d340ef8073736b1eb4098a
- 출처 데이터셋
- uspto-grants-1997_12
- 특허 번호
- US05703239
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