Benzamide, N-(4-hydroxybutyl)- → Indane-2-carboxylic acid-(4-hydroxybutyl)amide

반응식

[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH:2]1[C:10](Cl)=[O:11].[OH:13][CH2:14][CH2:15][CH2:16][CH2:17][NH:18]C(=O)C1C=CC=CC=1>>[OH:13][CH2:14][CH2:15][CH2:16][CH2:17][NH:18][C:10]([CH:2]1[CH2:3][C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH2:1]1)=[O:11]

참가 물질

반응물 2

HCID 11217773Benzamide, N-(4-hydroxybutyl)-

HCID 213133822,3-dihydro-1H-indene-2-carbonyl chloride

생성물 1

HCID 66937618Indane-2-carboxylic acid-(4-hydroxybutyl)amide수율 62%

실험 절차

Indane-2-carboxylic acid-(4-hydroxybutyl)amide (26B) is prepared from 26A as described for 1D.

출처 및 근거

ORD 기록: ord-f740e803a0074b52940ec335dcd79cee
출처 데이터셋: uspto-grants-2013_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08389555B2

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