4-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amide → 4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

HRID 1942373노트

반응식

HRID 1942373 반응식
C([O:3][CH:4](OCC)[CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:16][CH2:15][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH2:12]1)=[O:10])C.O=CCCCNC(C1CCCCC1)=O>>[O:3]=[CH:4][CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:12][CH2:13][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:15][CH2:16]1)=[O:10]

참가 물질

3

반응물 2

HCID 669375364-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amideHCID 85725969Cyclohexanecarboxylic acid (4-oxo-butyl)-amide

생성물 1

HCID 866513094-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

실험 절차

4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide (61C) is prepared from 61B as described for 20B. The product is obtained in almost quantitative yield.

후처리

  1. customThe product is obtained in almost quantitative yield

출처 및 근거

ORD 기록
ord-f3b89ee816344ddbbf4e68c4b58ff5cf
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08389555B2

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