Benzamide, N-(4-hydroxybutyl)- → 4-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide

HRID 1942376노트

반응식

HRID 1942376 반응식
[C:1]1([C:7]2[CH2:8][CH2:9][N:10]([C:13](Cl)=[O:14])[CH2:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH:16][CH2:17][CH2:18][CH2:19][CH2:20][NH:21]C(=O)C1C=CC=CC=1>>[OH:16][CH2:17][CH2:18][CH2:19][CH2:20][NH:21][C:13]([N:10]1[CH2:11][CH:12]=[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:8][CH2:9]1)=[O:14]

참가 물질

3

반응물 2

HCID 11217773Benzamide, N-(4-hydroxybutyl)-HCID 858108644-Phenyl-3,6-dihydro-2H-pyridine-1-carbonyl chloride

생성물 1

HCID 669374264-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide

실험 절차

4-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide (62B) is prepared from 62A as described for 1D. The product is obtained in almost quantitative yield.

후처리

  1. customThe product is obtained in almost quantitative yield

출처 및 근거

ORD 기록
ord-3d2647c7d9844d499a257e34f3032463
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08389555B2

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