3-Bromo-5-methylthiophene-2-carbaldehyde → 3-Benzenesulfonyl-5-methylthiophene-2-carbaldehyde

반응식

Br[C:2]1[CH:6]=[C:5]([CH3:7])[S:4][C:3]=1[CH:8]=[O:9].[Na+].[C:11]1([S:17]([O-:19])=[O:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([S:17]([C:2]2[CH:6]=[C:5]([CH3:7])[S:4][C:3]=2[CH:8]=[O:9])(=[O:19])=[O:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

반응물 2

HCID 8188853-Bromo-5-methylthiophene-2-carbaldehyde

HCID 2723840Benzenesulfinic acid, sodium salt

생성물 1

HCID 866522043-Benzenesulfonyl-5-methylthiophene-2-carbaldehyde

실험 절차

The title compound was prepared by the method of Preparation 7a using 3-bromo-5-methylthiophene-2-carbaldehyde and phenylsulfinic acid sodium salt.

출처 및 근거

ORD 기록: ord-66428ba1fc1c44309d8180e69a5e0c8c
출처 데이터셋: uspto-grants-2013_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08394836B2

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