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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 19458생성일: 2026년 10월 24일

Glutaric anhydride → 4-[(3-Ethynylphenyl)carbamoyl]butanoic acid

https://huagongshe.com/ko/reaction/19458

반응식

참여 물질

역할이름HCID투입량
반응물Glutaric anhydrideHCID 7940—
반응물Benzenamine, 3-ethynyl-HCID 104682—
용매DichloromethaneHCID 6344—
생성물4-[(3-Ethynylphenyl)carbamoyl]butanoic acidHCID 4352924099%

반응 단계

Glutaric anhydride (215 mg, 1.9 mmol) was dissolved in anhydrous dichloromethane (7 ml) and followed by the addition of 3-ethynylaniline (200 mg, 1.7 mmol). The mixture was allowed to stir at room temperature for 6 hours before the solvent was evaporated under reduced pressure to provide the product as a white solid (363 mg, 99%);

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07745229B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-b51d7cb6b41e41718e3f39d76b7da4bc
출처 메모uspto-grants-2010_06