Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178446226, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | HCID 178446227 | HCID 178446227 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178446226 | HCID 178446226 | — |
반응 단계
To a solution of tert-butyl 4-(cyclohexylamino)-2-oxo-1-pent-4-en-1-yl-1,3,8-triazaspiro[4.5]dec-3-ene-8-carboxylate (785 mg, 1.88 mmol) in DCM (2 mL) was added HCl (1.64 mL, 6.56 mmol, 4N dioxane). The reaction mixture was stirred at rt for 1 h, concentrated in vacuo, taken in DCM and concentrated in vacuo again, to provide the desired product LRMS (M+1)=319.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08399473B2 |
| 출처 데이터셋 | uspto-grants-2013_03 |
| ORD ID | ord-5b000049571d46719e27c2eccf9bbefb |
| 출처 메모 | uspto-grants-2013_03 |