3-Hydrazinylbenzonitrile--hydrogen chloride (1/1) → HCID 58277372, 화합물

HRID 1949222노트

반응식

HRID 1949222 반응식
Cl.[C:2]([C:4]1[CH:5]=[C:6]([NH:10][NH2:11])[CH:7]=[CH:8][CH:9]=1)#[N:3].ClC1C=C(N2[C:24]([C:25]3[CH:30]=[C:29]([F:31])[CH:28]=[C:27]([Cl:32])[CH:26]=3)=[CH:23][C:22]([C:33]([O:35][CH2:36][CH3:37])=[O:34])=N2)C=CC=1F>>[Cl:32][C:27]1[CH:26]=[C:25]([C:24]2[N:10]([C:6]3[CH:7]=[CH:8][CH:9]=[C:4]([C:2]#[N:3])[CH:5]=3)[N:11]=[C:22]([C:33]([O:35][CH2:36][CH3:37])=[O:34])[CH:23]=2)[CH:30]=[C:29]([F:31])[CH:28]=1

참가 물질

3

반응물 2

HCID 164953403-Hydrazinylbenzonitrile--hydrogen chloride (1/1)HCID 58277311HCID 58277311, 화합물

생성물 1

HCID 58277372HCID 58277372, 화합물

실험 절차

The preparation of the title compound takes place starting from the compound of Example 1A and 3-cyanophenylhydrazine hydrochloride in analogy to the synthesis of the compound of Example 21A. 1.96 g of the title compound with 55% purity (86% of theory) are obtained.

출처 및 근거

ORD 기록
ord-05b29c1e0db24e25b42f8e85d2e54a98
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08399682B2

반응 노트

불러오는 중…