4-Ethenylphenyl acetate → Acetic acid 4-[2-(2-amino-4-methoxyphenyl)vinyl]phenyl ester

HRID 1950127노트

반응식

HRID 1950127 반응식
Br[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][C:3]=1[N+:10]([O-])=O.[C:13]([O:16][C:17]1[CH:24]=[CH:23][C:20]([CH:21]=[CH2:22])=[CH:19][CH:18]=1)(=[O:15])[CH3:14]>>[NH2:10][C:3]1[CH:4]=[C:5]([O:8][CH3:9])[CH:6]=[CH:7][C:2]=1[CH:22]=[CH:21][C:20]1[CH:23]=[CH:24][C:17]([O:16][C:13](=[O:15])[CH3:14])=[CH:18][CH:19]=1

참가 물질

3

반응물 2

HCID 758214-Ethenylphenyl acetateHCID 792884-Bromo-3-nitroanisole

생성물 1

HCID 66627499Acetic acid 4-[2-(2-amino-4-methoxyphenyl)vinyl]phenyl ester

실험 절차

Synthesized from 4-bromo-3-nitroanisole (2.3 g) and 4-acetoxystyrene (1.7 ml) according to an analogous synthetic method to Example 107, the title compound (1.2 g) was obtained.

출처 및 근거

ORD 기록
ord-f5fc88592e25422db136e97187bb52ab
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08399520B2

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