2-Aminocyclohexanone → 2-Methylsulfanyl-N-(2-oxo-cyclohexyl)-4-trifluoromethyl-benzamide

HRID 1950894

반응식

HRID 1950894 반응식
[NH2:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C:3]1=[O:8].[CH3:9][S:10][C:11]1[CH:19]=[C:18]([C:20]([F:23])([F:22])[F:21])[CH:17]=[CH:16][C:12]=1[C:13](O)=[O:14]>>[CH3:9][S:10][C:11]1[CH:19]=[C:18]([C:20]([F:21])([F:22])[F:23])[CH:17]=[CH:16][C:12]=1[C:13]([NH:1][CH:2]1[CH2:7][CH2:6][CH2:5][CH2:4][C:3]1=[O:8])=[O:14]

참가 물질

3

반응물 2

HCID 4138882-AminocyclohexanoneHCID 11085762Benzoic acid, 2-(methylthio)-4-(trifluoromethyl)-2회

생성물 1

HCID 580629402-Methylsulfanyl-N-(2-oxo-cyclohexyl)-4-trifluoromethyl-benzamide

실험 절차

The title compound, off-white solid, MS: m/e=332.1 [(M+H)+], was prepared in accordance with the general method of intermediate B from 2-amino-cyclohexanone and 2-methylsulfanyl-4-trifluoromethyl-benzoic acid (intermediate C).

출처 및 근거

ORD 기록
ord-e2a32501af0748bdb980d801ccf555f8
출처 데이터셋
uspto-grants-2013_03
특허 번호
US08404673B2

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