Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Isopropylaniline → 2-[(2-Isopropyl)phenylamino]-isophthalic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Isopropylaniline | HCID 12561 | — |
| 반응물 | 2-Iodoisophthalic Acid | HCID 320100 | — |
| 생성물 | 2-[(2-Isopropyl)phenylamino]-isophthalic acid | HCID 10756554 | 38% |
반응 단계
Similar reaction of 2-iodoisophthalic acid and 2-isopropylaniline gave 2-[(2-isopropyl)phenylamino]-isophthalic acid (38%), mp (EtOAc/petroleum ether) 217-219° C. 1H NMR [(CD3)2SO] δ 1.25 (d, J=6.8 Hz, 6 H, 2×CH3), 3.22-3.29 (m, 1 H, CH), 6.81 (dd, J=7.4, 1.8 Hz, 1 H, H-3' or H-6'), 6.93 (t, J=7.7 Hz, 1 H, H-2), 6.92-7.02 (m, 2 H, H-4' and H-5'), 7.26 (dd, J=7.1, 2.2 Hz, 1 H, H-6' or H-3'), 7.90 (d, J=7.7 Hz, 2 H, H-4 and H-6), 9.69 (s, 1 H, NH), 12.93 (br s, 2 H, 2×COOH). Anal. (C17H17NO4) C, H, N.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06114332 |
| 출처 데이터셋 | uspto-grants-2000_09 |
| ORD ID | ord-016d126452e54a86a3bc93467d7a1ded |
| 출처 메모 | uspto-grants-2000_09 |