Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Tert-Butylaniline → 2-[(4-Tert-butyl)phenylamino]isophthalic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Tert-Butylaniline | HCID 69861 | — |
| 반응물 | 2-Iodoisophthalic Acid | HCID 320100 | — |
| 생성물 | 2-[(4-Tert-butyl)phenylamino]isophthalic acid | HCID 10638910 | 93% |
반응 단계
Similar reaction of 2-iodoisophthalic acid and 4-tert-butylaniline gave 2-[(4-tert-butyl)phenylamino]isophthalic acid (93%), mp (EtOAc/petroleum ether) 221-222° C. 1H NMR [(CD3)2SO] δ 1.24 (s, 9 H, 3×CH3), 6.84 (d, J=8.7 Hz, 2 H, H-2' and H-6' or H-3' and H-5'), 6.99 (t, J=7.7 Hz, 1 H, H-5), 7.21 (d, J=8.6 Hz, 2 H, H-3' and H-5' or H-2' and H-6'), 7.93 (d, J=7.8 Hz, 2 H, H-4 and H-6), 9.65 (br s, 1 H, NH) and 12.99 (br s, 2 H, 2×COOH Anal. (C18H13NO2) C, H, N.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06114332 |
| 출처 데이터셋 | uspto-grants-2000_09 |
| ORD ID | ord-2b320f6004814090b5fea3da16316eac |
| 출처 메모 | uspto-grants-2000_09 |