p-Toluenesulfonic acid monohydrate → 2-isopropylidene-1-indanone

HRID 1953947노트

반응식

HRID 1953947 반응식
[OH2:1].[C:2]1([CH3:12])[CH:7]=[CH:6][C:5](S(O)(=O)=O)=[CH:4][CH:3]=1>C1C=CC=CC=1>[C:2](=[C:3]1[CH2:4][C:7]2[C:2](=[CH:3][CH:4]=[CH:5][CH:6]=2)[C:12]1=[O:1])([CH3:12])[CH3:7]

참가 물질

3

반응물 1

HCID 521998p-Toluenesulfonic acid monohydrate

생성물 1

HCID 15133342-isopropylidene-1-indanone

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

The reaction mixture was dissolved in 300 ml of benzene and 4.2 g of p-toluenesulfonic acid monohydrate was added to the solution and refluxed for 2 hours for component distillation. The product was used in the subsequent reaction without purification.

후처리

  1. temperaturerefluxed for 2 hours for component distillation
  2. customThe product was used in the subsequent reaction without purification

출처 및 근거

ORD 기록
ord-ec9a2c624181455a96b4fab23f811200
출처 데이터셋
uspto-grants-2000_09
특허 번호
US06121182

반응 노트

불러오는 중…