Phenyl isocyanate → HCID 22390756, 화합물

HRID 1956355노트

반응식

HRID 1956355 반응식
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[C:8]1([N:14]=[C:15]=[O:16])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>C(Cl)Cl>[CH:11]1[CH:12]=[CH:13][C:8]([NH:14][C:15]([N:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4])=[O:16])=[CH:9][CH:10]=1

참가 물질

4

반응물 2

HCID 7672Phenyl isocyanateHCID 8113Diethanolamine

생성물 1

HCID 22390756HCID 22390756, 화합물수율 119.7%

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

실험 절차

A mixture of 15.62 ml (0.136 mol) of diethanolamine and 163 ml of methylene chloride is poured, at a temperature of 10° C., into a three-necked flask containing 18.25 ml (0.168 mol) of phenyl isocyanate dissolved in 37 ml of CH2Cl2. The mixture is left at that temperature for one hour, and then at room temperature overnight, and concentrated in vacuo to obtain 36.5 g of the expected product. (Yield=100%).

후처리

  1. additionis poured, at a temperature of 10° C., into a three-necked flask
  2. concentrationat room temperature overnight, and concentrated in vacuo

출처 및 근거

ORD 기록
ord-4479d36f66b044a8b02785945fd15504
출처 데이터셋
uspto-grants-1998_07
특허 번호
US05780474

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