Methyl Thioglycolate → HCID 849403, 화합물

HRID 1957204노트

반응식

HRID 1957204 반응식
[C:1]1([N:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9]([CH:16]=O)=[C:8]2Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[SH:19][CH2:20][C:21]([O:23][CH3:24])=[O:22]>>[C:1]1([N:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9]3[CH:16]=[C:20]([C:21]([O:23][CH3:24])=[O:22])[S:19][C:8]2=3)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

3

반응물 2

HCID 16907Methyl ThioglycolateHCID 3147932-chloro-1-phenyl-1H-indole-3-carbaldehyde

생성물 1

HCID 849403HCID 849403, 화합물수율 79.6%

실험 절차

Prepared from 1-Phenyl-2-chloroindole-3-carbaldehyde (0.90 g), K2 CO3 (1.38 g) and methyl 2-mercaptoacetate (0.55 ml) yielding (51) 0.86 g (79.6%). M.p. 147°-149° C.

출처 및 근거

ORD 기록
ord-ae0b0339738147deaf015c6ae6eeddfa
출처 데이터셋
uspto-grants-1998_07
특허 번호
US05783575

반응 노트

불러오는 중…