참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethylene Oxide | HCID 6354 | — |
| 반응물 | N-Methyloctadecylamine | HCID 75539 | — |
| 생성물 | N-(2-hydroxyethyl)-N-methyl-octadecylamine | HCID 13564486 | 86.6% |
반응 단계
An autoclave provided with a stirrer, a thermometer, a pressure gauge and a pressure dropping funnel was charged with 250 g of N-methyloctadecylamine and heated to 160° C. Then 45 g of ethylene oxide was occasionally added dropwise thereto under a pressure of 0 to 6 kg/cm2G. Three hours were required for completing the addition. Next, the resulting mixture was aged, i.e., maintained, at 160° C. for 2 hours and then cooled. The reaction mixture was taken out and distilled to thereby give 250 g of N-(2-hydroxyethyl)-N-methyloctadecylamine. This product had a boiling point of 185° to 190° C./0.2 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05728649 |
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| 출처 데이터셋 | uspto-grants-1998_03 |
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| ORD ID | ord-dd6d1a78ee72419a8409d1047d1e9c38 |
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| 출처 메모 | uspto-grants-1998_03 |
|---|