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Potassium Carbonate → N,N-dimethyl-2-(4-nitro-1H-pyrazol-1-yl)ethanamine

HRID 1968520
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인쇄 미리보기

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HRID 1968520 반응식
Cl.[CH3:2][N:3]([CH3:7])[CH2:4][CH2:5]Cl.C(=O)([O-])[O-].[K+].[K+].[N+:14]([C:17]1[CH:18]=[N:19][NH:20][CH:21]=1)([O-:16])=[O:15]>CC(C)=O>[CH3:2][N:3]([CH3:7])[CH2:4][CH2:5][N:19]1[CH:18]=[C:17]([N+:14]([O-:16])=[O:15])[CH:21]=[N:20]1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 163764-nitro-1H-pyrazoleHCID 11636816N,N-Dimethylaminoethyl chloride hydrochloride

생성물 1

HCID 56777237N,N-dimethyl-2-(4-nitro-1H-pyrazol-1-yl)ethanamine

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

2-Dimethylaminoethyl chloride hydrochloride (955 mg, 6.63 mmol), potassium carbonate (1.83 g, 8.84 mmol) and 4-nitro-1H-pyrazole (750 mg, 6.63 mmol) were combined in acetone (30 ml) and the reaction was stirred overnight at reflux. After cooling to room temperature, the crude reaction mixture was filtered to remove inorganics, and the filtrate was concentrated to give the product.

후처리

  1. temperatureat reflux
  2. customthe crude reaction mixture
  3. filtrationwas filtered
  4. customto remove inorganics
  5. concentrationthe filtrate was concentrated
  6. customto give the product

출처 및 근거

ORD 기록
ord-90cd9357aed94eada62ef2c2cd7b9c0b
출처 데이터셋
uspto-grants-2013_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08426408B2

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