Tert-Butylamine → HCID 58124811, 화합물
반응식
CS(O[CH2:6][CH2:7][CH2:8][C:9]#[C:10][C:11]1[S:12][CH:13]=[CH:14][CH:15]=1)(=O)=O.[C:16]([NH2:20])([CH3:19])([CH3:18])[CH3:17]>>[C:16]([NH:20][CH2:6][CH2:7][CH2:8][C:9]#[C:10][C:11]1[S:12][CH:13]=[CH:14][CH:15]=1)([CH3:19])([CH3:18])[CH3:17]참가 물질
3
실험 절차
A mixture of 210 mg of 2b and 5 ml of tert-butyl amine was stirred for 4 days. The reaction mixture was concentrated and the residue was treated with 20 ml of 1M K2CO3 and the product was extracted into ethyl acetate. The organic layer was washed once with water, dried and concentrated, to provide 250 mg of 2c as a colorless oil.
후처리
- concentrationThe reaction mixture was concentrated
- additionthe residue was treated with 20 ml of 1M K2CO3
- extractionthe product was extracted into ethyl acetate
- washThe organic layer was washed once with water
- customdried
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-8e0de67fab5d417e84bc9474c78ac7a0
- 출처 데이터셋
- uspto-grants-2013_04
- 특허 번호
- US08431564B2
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