참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phthalic Anhydride | HCID 6811 | — |
| 반응물 | (2-Amino-2,3-dihydro-1H-inden-2-yl)methanol | HCID 22080542 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-(2-Hydroxymethylindan-2-yl)-isoindole-1,3-dione | HCID 68561206 | — |
반응 단계
A mixture of (2-aminoindan-2-yl)methanol (0.407 g, 2.50 mmol) and phthalic anhydride (0.369 g, 2.50 mmol) is heated at 160° C. for 40 minutes. The reaction mixture is poured into water and extracted with chloroform. The organic phase is dried (Na2SO4) and evaporated to afford 2-(2-hydroxymethylindan-2-yl)-isoindole-1,3-dione, MH+294.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07745462B2 |
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| 출처 데이터셋 | uspto-grants-2010_06 |
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| ORD ID | ord-9c2a51c334da45ef9b380da3998da7ac |
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| 출처 메모 | uspto-grants-2010_06 |
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