Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Benzyl-6-bromo-2H-indazole → 2-Benzyl-6-chloro-5-fluoro-2H-indazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Benzyl-6-bromo-2H-indazole | HCID 58529689 | — |
| 반응물 | 6-chloro-5-fluoro-1H-indazole | HCID 58529904 | — |
| 생성물 | 2-Benzyl-6-chloro-5-fluoro-2H-indazole | HCID 58529592 | — |
반응 단계
This compound was prepared in a manner similar to the procedure described for the preparation of 2-benzyl-6-bromo-2H-indazole, using 6-chloro-5-fluoro-1H-indazole in place of 6-bromoindazole. 1H-NMR (300 MHz, DMSO-d6) 8.54 (s, 1H), 7.90 (d, 1H), 7.71 (d, 1H), 7.36 to 7.29 (m, 5H), 5.64 (s, 2H); ES-MS m/z 261.0 [M+H]+, RT (min) 3.56.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08431695B2 |
| 출처 데이터셋 | uspto-grants-2013_04 |
| ORD ID | ord-08504bf612ff4d49958303b44747c49d |
| 출처 메모 | uspto-grants-2013_04 |